SEM-EDS data of geological and archaeological sample analysis (doi:10.57979/K3OBDC)

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Part 2: Study Description
Part 3: Data Files Description
Part 4: Variable Description
Part 5: Other Study-Related Materials
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SEM-EDS data of geological and archaeological sample analysis

doi:10.57979/K3OBDC

POLEN DataHub

2026-05-13

1

Neto Belmiro, Joana Filipa, 2026, "SEM-EDS data of geological and archaeological sample analysis", https://doi.org/10.57979/K3OBDC, POLEN DataHub, V1, UNF:6:R7fUX8XwI0jeIEztHbKwYg== [fileUNF]

SEM-EDS data of geological and archaeological sample analysis

doi:10.57979/K3OBDC

Neto Belmiro, Joana Filipa (Universidade do Algarve)

Joana Filipa Neto Belmiro

2026-05-01

2020/08722/BD

POLEN DataHub

Neto Belmiro, Joana Filipa

Neto Belmiro, Joana Filipa

2026-05-01

https://doi.org/10.57979/K3OBDC

Humanities - History and Archaeology - Archaeology, SEM-EDS, SEM, EDS, EDS – mapping, EDS – spectra

Polished chips of geological and archaeological samples were analysed with a variable pressure Hitachi S3700N SEM, coupled with a Quantax EDS microanalysis system at the HERCULES laboratory (University of Évora). Specifically, the Quantax system is equipped with a Bruker AXS 5010 XFlash Silicon Drift Detector, which offers a spectral resolution of 129 eV at FWHM for MnKα. The EDS elemental analysis and quantification were carried out with the ESPRIT software by Bruker. SEM-EDS obtained two types of data: 1) SEM - Microphotographs obtained through surface sample scanning; 2) EDS - Elemental composition data obtained through sample mapping or spectra acquired from specific points within the sample. The geological samples are chert samples from the Algarve basin, previously studied and described in Belmiro et al. (2023). The samples can also be consulted in our online reference collection (www.lusolit.icarehb.com). The archaeological samples include several chert types identified in the Upper Paleolithic sequence of the Vale Boi site, previously studied and described in Belmiro et al. (2025a,b).

STRUCTURE: The raw data are organised by data type and sample. - EDS_map_data: Spectra of specific points within the imaged area. Data: PNG image with the points measure within the sample (e.g., SP10(M4_1)Spectra1 with crosshairs 1, 2); SPX raw data file with analysis metadata; XLSX file with analysis specifications and spectrum results. SPX and XLSX files correspond to each individual spectrum identified in the PNG image (e.g., SP10(M4_1)Spectra1_1 and SP10(M4_1)Spectra1_2) - EDS_map_data: Elemental mapping of sample area. Data: BMP/TIFF with distribution of elements in the imaged area. Ch1 corresponds to the imaged area without elemental mapping; Ch1_*-K or Ch*- Kα correspond to the elemental mapping, showing one map for each chemical element according to the elemental table; - SEM_microphotographs: Microphotographs obtained through surface sample scanning. Data: TIFF microphotographs of sample areas; TXT files with metadata related to each TIFF microphotograph.

<a href="http://creativecommons.org/licenses/by-nc/4.0">CC BY-NC 4.0</a>

Belmiro, J. (2025). The exploitation of siliceous raw materials during the Upper Paleolithic in the southwest of the Iberian Peninsula.

10400.1/28422

Belmiro, J. (2025). The exploitation of siliceous raw materials during the Upper Paleolithic in the southwest of the Iberian Peninsula.

Belmiro, J., Terradas, X., & Cascalheira, J. (2023). Creating frames of reference for chert exploitation during the Late Pleistocene in Southwesternmost Iberia. PLOS ONE, 18(10).

10.1371/journal.pone.0293223

Belmiro, J., Terradas, X., & Cascalheira, J. (2023). Creating frames of reference for chert exploitation during the Late Pleistocene in Southwesternmost Iberia. PLOS ONE, 18(10).

Belmiro, J., Terradas, X., Dominguez-Bella, S., & Cascalheira, J. (2025). Within and Beyond: Chert Procurement Patterns During The Upper Palaeolithic in Southwesternmost Iberia. Journal of Paleolithic Archaeology, 8(1), 8.

10.1007/s41982-025-00209-2

Belmiro, J., Terradas, X., Dominguez-Bella, S., & Cascalheira, J. (2025). Within and Beyond: Chert Procurement Patterns During The Upper Palaeolithic in Southwesternmost Iberia. Journal of Paleolithic Archaeology, 8(1), 8.

Belmiro, J., Bicho, N., Terradas, X., & Cascalheira, J. (2025). From stone to tool: How raw materials influenced Upper Palaeolithic technology in southwestern Iberia (Vale Boi). Archaeological and Anthropological Sciences, 17(11), 220.

10.1007/s12520-025-02339-8

Belmiro, J., Bicho, N., Terradas, X., & Cascalheira, J. (2025). From stone to tool: How raw materials influenced Upper Palaeolithic technology in southwestern Iberia (Vale Boi). Archaeological and Anthropological Sciences, 17(11), 220.

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Ch 1-1.bmp

Text:

image/bmp

Label:

Ch 1.bmp

Text:

image/bmp

Label:

Ch 1_C-K-1.bmp

Text:

image/bmp

Label:

Ch 1_C-K.bmp

Text:

image/bmp

Label:

Ch 1_Ca-Kα-1.bmp

Text:

image/bmp

Label:

Ch 1_Ca-Kα.bmp

Text:

image/bmp

Label:

Ch 1_Fe-Kα-1.bmp

Text:

image/bmp

Label:

Ch 1_Fe-Kα.bmp

Text:

image/bmp

Label:

Ch 1_K-Kα-1.bmp

Text:

image/bmp

Label:

Ch 1_K-Kα.bmp

Text:

image/bmp

Label:

Ch 1_O-K-1.bmp

Text:

image/bmp

Label:

Ch 1_O-K.bmp

Text:

image/bmp

Label:

Ch 1_P-Kα-1.bmp

Text:

image/bmp

Label:

Ch 1_P-Kα.bmp

Text:

image/bmp

Label:

Ch 1_S-Kα-1.bmp

Text:

image/bmp

Label:

Ch 1_S-Kα.bmp

Text:

image/bmp

Label:

Ch 1_Si-Kα.bmp

Text:

image/bmp

Label:

Ch 1-1.bmp

Text:

image/bmp

Label:

Ch 1.bmp

Text:

image/bmp

Label:

Ch 1_Al-K-1.bmp

Text:

image/bmp

Label:

Ch 1_Al-K.bmp

Text:

image/bmp

Label:

Ch 1_C-K.bmp

Text:

image/bmp

Label:

Ch 1_Ca-Kα-1.bmp

Text:

image/bmp

Label:

Ch 1_Ca-Kα.bmp

Text:

image/bmp

Label:

Ch 1_Fe-Kα-1.bmp

Text:

image/bmp

Label:

Ch 1_Fe-Kα.bmp

Text:

image/bmp

Label:

Ch 1_K-Kα-1.bmp

Text:

image/bmp

Label:

Ch 1_K-Kα.bmp

Text:

image/bmp

Label:

Ch 1_Na-K-1.bmp

Text:

image/bmp

Label:

Ch 1_Na-K.bmp

Text:

image/bmp

Label:

Ch 1_O-K-1.bmp

Text:

image/bmp

Label:

Ch 1_O-K.bmp

Text:

image/bmp

Label:

Ch 1_P-Kα.bmp

Text:

image/bmp

Label:

Ch 1_S-Kα-1.bmp

Text:

image/bmp

Label:

Ch 1_S-Kα.bmp

Text:

image/bmp

Label:

Ch 1_Si-Kα-1.bmp

Text:

image/bmp

Label:

Ch 1_Si-Kα.bmp

Text:

image/bmp

Label:

Ch 1-1.bmp

Text:

image/bmp

Label:

Ch 1.bmp

Text:

image/bmp

Label:

Ch 1_Al-K-1.bmp

Text:

image/bmp

Label:

Ch 1_Al-K.bmp

Text:

image/bmp

Label:

Ch 1_C-K.bmp

Text:

image/bmp

Label:

Ch 1_Ca-Kα-1.bmp

Text:

image/bmp

Label:

Ch 1_Ca-Kα.bmp

Text:

image/bmp

Label:

Ch 1_Fe-Kα-1.bmp

Text:

image/bmp

Label:

Ch 1_Fe-Kα.bmp

Text:

image/bmp

Label:

Ch 1_K-Kα-1.bmp

Text:

image/bmp

Label:

Ch 1_K-Kα.bmp

Text:

image/bmp

Label:

Ch 1_Na-K-1.bmp

Text:

image/bmp

Label:

Ch 1_Na-K.bmp

Text:

image/bmp

Label:

Ch 1_O-K-1.bmp

Text:

image/bmp

Label:

Ch 1_O-K.bmp

Text:

image/bmp

Label:

Ch 1_P-Kα-1.bmp

Text:

image/bmp

Label:

Ch 1_P-Kα.bmp

Text:

image/bmp

Label:

Ch 1_S-Kα-1.bmp

Text:

image/bmp

Label:

Ch 1_S-Kα.bmp

Text:

image/bmp

Label:

Ch 1_Si-Kα.bmp

Text:

image/bmp

Label:

Ch 1-1.bmp

Text:

image/bmp

Label:

Ch 1.bmp

Text:

image/bmp

Label:

Ch 1_Al-K-1.bmp

Text:

image/bmp

Label:

Ch 1_Al-K.bmp

Text:

image/bmp

Label:

Ch 1_C-K-1.bmp

Text:

image/bmp

Label:

Ch 1_C-K.bmp

Text:

image/bmp

Label:

Ch 1_Fe-Kα-1.bmp

Text:

image/bmp

Label:

Ch 1_Fe-Kα.bmp

Text:

image/bmp

Label:

Ch 1_O-K-1.bmp

Text:

image/bmp

Label:

Ch 1_O-K.bmp

Text:

image/bmp

Label:

Ch 1_Si-Kα-1.bmp

Text:

image/bmp

Label:

Ch 1_Si-Kα.bmp

Text:

image/bmp

Label:

Ch 1.bmp

Text:

image/bmp

Label:

Ch 1_Al-K-1.bmp

Text:

image/bmp

Label:

Ch 1_Al-K.bmp

Text:

image/bmp

Label:

Ch 1_C-K-1.bmp

Text:

image/bmp

Label:

Ch 1_C-K.bmp

Text:

image/bmp

Label:

Ch 1_Ca-Kα.bmp

Text:

image/bmp

Label:

Ch 1_Fe-Kα.bmp

Text:

image/bmp

Label:

Ch 1_K-Kα.bmp

Text:

image/bmp

Label:

Ch 1_O-K-1.bmp

Text:

image/bmp

Label:

Ch 1_O-K.bmp

Text:

image/bmp

Label:

Ch 1_P-Kα-1.bmp

Text:

image/bmp

Label:

Ch 1_P-Kα.bmp

Text:

image/bmp

Label:

Ch 1_Si-Kα-1.bmp

Text:

image/bmp

Label:

Ch 1_Si-Kα.bmp

Text:

image/bmp

Label:

Ch 1-1.bmp

Text:

image/bmp

Label:

Ch 1.bmp

Text:

image/bmp

Label:

Ch 1_Al-K-1.bmp

Text:

image/bmp

Label:

Ch 1_Al-K.bmp

Text:

image/bmp

Label:

Ch 1_C-K-1.bmp

Text:

image/bmp

Label:

Ch 1_C-K.bmp

Text:

image/bmp

Label:

Ch 1_Ca-Kα.bmp

Text:

image/bmp

Label:

Ch 1_Cr-Kα-1.bmp

Text:

image/bmp

Label:

Ch 1_Cr-Kα.bmp

Text:

image/bmp

Label:

Ch 1_Fe-Kα-1.bmp

Text:

image/bmp

Label:

Ch 1_Fe-Kα.bmp

Text:

image/bmp

Label:

Ch 1_Mg-K-1.bmp

Text:

image/bmp

Label:

Ch 1_Mg-K.bmp

Text:

image/bmp

Label:

Ch 1_O-K-1.bmp

Text:

image/bmp

Label:

Ch 1_O-K.bmp

Text:

image/bmp

Label:

Ch 1_P-Kα-1.bmp

Text:

image/bmp

Label:

Ch 1_P-Kα.bmp

Text:

image/bmp

Label:

Ch 1_Si-Kα-1.bmp

Text:

image/bmp

Label:

Ch 1_Si-Kα.bmp

Text:

image/bmp

Label:

Ch 1-1.bmp

Text:

image/bmp

Label:

Ch 1.bmp

Text:

image/bmp

Label:

Ch 1_Al-K-1.bmp

Text:

image/bmp

Label:

Ch 1_Al-K.bmp

Text:

image/bmp

Label:

Ch 1_C-K-1.bmp

Text:

image/bmp

Label:

Ch 1_C-K.bmp

Text:

image/bmp

Label:

Ch 1_Ca-Kα.bmp

Text:

image/bmp

Label:

Ch 1_Cl-Kα-1.bmp

Text:

image/bmp

Label:

Ch 1_Cl-Kα.bmp

Text:

image/bmp

Label:

Ch 1_Fe-Kα-1.bmp

Text:

image/bmp

Label:

Ch 1_Fe-Kα.bmp

Text:

image/bmp

Label:

Ch 1_K-Kα-1.bmp

Text:

image/bmp

Label:

Ch 1_K-Kα.bmp

Text:

image/bmp

Label:

Ch 1_O-K-1.bmp

Text:

image/bmp

Label:

Ch 1_O-K.bmp

Text:

image/bmp

Label:

Ch 1_P-Kα-1.bmp

Text:

image/bmp

Label:

Ch 1_P-Kα.bmp

Text:

image/bmp

Label:

Ch 1_S-Kα-1.bmp

Text:

image/bmp

Label:

Ch 1_S-Kα.bmp

Text:

image/bmp

Label:

Ch 1_Si-Kα-1.bmp

Text:

image/bmp

Label:

Ch 1_Si-Kα.bmp

Text:

image/bmp

Label:

Ch 1_Ti-Kα-1.bmp

Text:

image/bmp

Label:

Ch 1_Ti-Kα.bmp

Text:

image/bmp

Label:

Ch 1-1.bmp

Text:

image/bmp

Label:

Ch 1.bmp

Text:

image/bmp

Label:

Ch 1_Al-K-1.bmp

Text:

image/bmp

Label:

Ch 1_Al-K.bmp

Text:

image/bmp

Label:

Ch 1_C-K-1.bmp

Text:

image/bmp

Label:

Ch 1_C-K.bmp

Text:

image/bmp

Label:

Ch 1_Ca-Kα-1.bmp

Text:

image/bmp

Label:

Ch 1_Ca-Kα.bmp

Text:

image/bmp

Label:

Ch 1_Cl-Kα-1.bmp

Text:

image/bmp

Label:

Ch 1_Cl-Kα.bmp

Text:

image/bmp

Label:

Ch 1_Fe-Kα-1.bmp

Text:

image/bmp

Label:

Ch 1_Fe-Kα.bmp

Text:

image/bmp

Label:

Ch 1_O-K-1.bmp

Text:

image/bmp

Label:

Ch 1_O-K.bmp

Text:

image/bmp

Label:

Ch 1_P-Kα-1.bmp

Text:

image/bmp

Label:

Ch 1_P-Kα.bmp

Text:

image/bmp

Label:

Ch 1_S-Kα-1.bmp

Text:

image/bmp

Label:

Ch 1_S-Kα.bmp

Text:

image/bmp

Label:

Ch 1_Si-Kα-1.bmp

Text:

image/bmp

Label:

Ch 1_Si-Kα.bmp

Text:

image/bmp

Label:

Ch 1_Ti-Kα-1.bmp

Text:

image/bmp

Label:

Ch 1_Ti-Kα.bmp

Text:

image/bmp

Label:

Ch 1.bmp

Text:

image/bmp

Label:

Ch 1_Al-K.bmp

Text:

image/bmp

Label:

Ch 1_C-K-1.bmp

Text:

image/bmp

Label:

Ch 1_C-K.bmp

Text:

image/bmp

Label:

Ch 1_Fe-Kα-1.bmp

Text:

image/bmp

Label:

Ch 1_Fe-Kα.bmp

Text:

image/bmp

Label:

Ch 1_K-Kα.bmp

Text:

image/bmp

Label:

Ch 1_O-K-1.bmp

Text:

image/bmp

Label:

Ch 1_O-K.bmp

Text:

image/bmp

Label:

Ch 1_P-Kα-1.bmp

Text:

image/bmp

Label:

Ch 1_P-Kα.bmp

Text:

image/bmp

Label:

Ch 1_Si-Kα-1.bmp

Text:

image/bmp

Label:

Ch 1_Si-Kα.bmp

Text:

image/bmp

Label:

Ch 1_Ti-Kα.bmp

Text:

image/bmp

Label:

Ch 1-1.bmp

Text:

image/bmp

Label:

Ch 1.bmp

Text:

image/bmp

Label:

Ch 1_Al-K-1.bmp

Text:

image/bmp

Label:

Ch 1_Al-K.bmp

Text:

image/bmp

Label:

Ch 1_C-K-1.bmp

Text:

image/bmp

Label:

Ch 1_C-K.bmp

Text:

image/bmp

Label:

Ch 1_Ca-Kα-1.bmp

Text: